Custom CDS pyroprobe with autosampler coupled to homebuilt packed bed reactor. Reactor has 6 port valves to allow for either pulses or continuous flow of model compounds into the packed bed reactor. Vapor stream enters Shimdazu GC split to both MS and FID detectors. Light gases are quantified with online MKS MS connected to vent line.
Access to 7 plug flow reactors coupled to a GC-FID capable of operating at atmospheric or high pressure.
Three fluidized bed reactors coupled with mass flow controllers and syringe pump injection ports for carbon nanotube synthesis. One of the reactors is designed for high pressure operation.
For nanotube and graphene growth on wafers
We have access to 11 Parr autoclave reactors, each coupled with mass flow controllers, pressure relief valves, refrigerated recirculators, and a pressure regulator.
Coupled with online MKS mass spec and mass flow controllers to quantify gas phase products. System is housed in a tinted UV blocking ventilated enclosure, cooled with a refrigerated recirculating bath.
with ATR-IR+UV-VIS+Raman probes with limits of 573K and 35 bar
TGA with DSC
XRD
Calorimeter with connection to ASAP 2020 dosing system for heat of adsorption measurements and puncture cell for heat of immersion measurements
TP units coupled with methanator + FID detector for TPO, and TCD detector for TPR runs
XPS
FTIR 1 with reaction cell
FTIR 2 with ATR and TGA interface
Shimadzu GCMS with autosampler
Raman
Agilent GCMS
UV-VIS
Adsorption system 1
Adsorption system 2
